N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

Base Information

Chemical Name:N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester
CAS No.:158975-47-4
Molecular Formula:C₄₆H₄₁NO₁₄
Molecular Weight:831.83
Hs Code.:

Synonyms:N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

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Chemical Property of N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

Chemical Property:

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Technology Process of N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

There total 1 articles about N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.9%

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 158975-47-4
N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(94)84227-2

Reference yield: 60.7%

: 158975-47-4
N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

: 159098-98-3
N-(carbobenzoxy)-α-D-mannopyranosyl-(1<*>3)-L-serine methyl ester

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 6.5h;
DOI:10.1016/0008-6215(94)84227-2

Reference yield:

: 158975-47-4
N-(carbobenzoxy)-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

: 158975-42-9
N-(carbobenzoxy)-(2,3,4-tri-O-acetyl-α-D-mannopyranosyl)-(1<*>3)-L-serine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 60.7 percent / NaOMe / methanol / 6.5 h / 0 °C

2: pyridine / 30 h / 70 °C

3: pyridine / 0 - 20 °C

4: 87 percent / 80percent aq. AcOH / 6 h / 55 °C

With pyridine; sodium methylate; acetic acid; In methanol;
DOI:10.1016/0008-6215(94)84227-2