2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde

Base Information

• Chemical Name: 2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde
• CAS No.: 1264244-23-6
• Molecular Formula: C₂₁H₂₉NO₂
• Molecular Weight: 327.467

Synonyms:2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde

Chemical Property of 2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of 2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde

There total 1 articles about 2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[1'-(cyclohexylmethyl)-3H-spiro[[2]-benzoxepine-1,4'-piperidin]-3-yl-oxy]ethanol (1264244-40-7) → 2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde (1264244-23-6)

Guidance literature:

2-[1'-(cyclohexylmethyl)-3H-spiro[[2]-benzoxepine-1,4'-piperidin]-3-yl-oxy]ethanol; With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 1.75h; Reflux;

With sodium hydroxide; In tetrahydrofuran; water;

DOI:10.1016/j.bmc.2010.11.013

Reference yield:

2-[1'-(cyclohexylmethyl)-3H-spiro[[2]benzofuran-1,4'-piperidin]-3-yl]acetaldehyde (1264244-23-6) → WMS-1832 (1265916-83-3)

Guidance literature:

With sodium tetrahydroborate; In acetonitrile; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.bmc.2010.11.013

upstream raw materials:

2-[1'-(cyclohexylmethyl)-3H-spiro[[2]-benzoxepine-1,4'-piperidin]-3-yl-oxy]ethanol

Downstream raw materials:

WMS-1832

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