(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

Base Information

Chemical Name:(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone
CAS No.:161553-25-9
Molecular Formula:C₁₇H₁₆F₃N₅O₃
Molecular Weight:395.341
Hs Code.:

Synonyms:(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

Chemical Property:

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Technology Process of (S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

There total 3 articles about (S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 38956-80-8
3-hydrazino-6-phenylpyridazine

: 161553-20-4
(S)-N-trifluoroacetyl-3-formylalanine methyl ester

: 161553-25-9
(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

Guidance literature:: With acetic acid; In methanol; for 1h; Ambient temperature;
DOI:10.1002/jhet.5570310524

Reference yield:

: 64881-40-9
(3S)-3-methoxycarbonyl-3-trifluoroacetylaminopropanoyl chloride

: 161553-25-9
(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂ / 10percent Pd/C / benzene / 5 h / Heating

2: 74 percent / AcOH / methanol / 1 h / Ambient temperature

With hydrogen; acetic acid; palladium on activated charcoal; In methanol; benzene;
DOI:10.1002/jhet.5570310524

Reference yield:

: 657-19-2
(S)-N-trifluoroacetylaspartic acid-1-methyl ester

: 161553-25-9
(S)-N-trifluoroacetyl-3-formylalanine methylester-(6-phenyl-3-pyridazinyl)hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 1 h / 60 - 70 °C / Heating

2: 96 percent / H₂ / 10percent Pd/C / benzene / 5 h / Heating

3: 74 percent / AcOH / methanol / 1 h / Ambient temperature

With thionyl chloride; hydrogen; acetic acid; palladium on activated charcoal; In methanol; benzene;
DOI:10.1002/jhet.5570310524