methyl 5-cyclohexa-1,3-diene-1-carboxylate

Base Information

Chemical Name:methyl 5-cyclohexa-1,3-diene-1-carboxylate
CAS No.:145264-64-8
Molecular Formula:C₁₄H₂₁NO₄
Molecular Weight:267.325
Hs Code.:

methyl 5-<N-(t-butoxycarbonyl)aminomethyl>cyclohexa-1,3-diene-1-carboxylate

Synonyms:methyl 5-cyclohexa-1,3-diene-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5-cyclohexa-1,3-diene-1-carboxylate

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Technology Process of methyl 5-cyclohexa-1,3-diene-1-carboxylate

There total 1 articles about methyl 5-cyclohexa-1,3-diene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79356-98-2
1-tert-Butoxycarbonyl-1,2-dihydropyridine

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 145264-64-8
methyl 5-cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: With lithium hexamethyldisilazane; Yield given. Multistep reaction; 1.) toluene, reflux, 2 d, 2.) THF, a) -78 deg C, 10 min, b) -78 -> 20 deg C;
DOI:10.1016/S0040-4020(01)89449-7

Reference yield: 85.0%

: 145264-64-8
methyl 5-cyclohexa-1,3-diene-1-carboxylate

: 134039-44-4
methyl 5-(aminomethyl)cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: With trifluoroacetic acid; for 0.0833333h;
DOI:10.1016/S0040-4020(01)89449-7

Reference yield: 39.0%

: 145264-64-8
methyl 5-cyclohexa-1,3-diene-1-carboxylate

: 145214-85-3,145264-65-9
methyl 3α,4α-dihydroxy-5β-cyclohex-1-ene-1-carboxylate

: 145214-85-3,145264-65-9
methyl 3β,4β-dihydroxy-5β-cyclohex-1-ene-1-carboxylate

Guidance literature:: With 4-methylmorpholine N-oxide; osmium(VIII) oxide; In water; acetone; tert-butyl alcohol; at 20 ℃; for 48h;
DOI:10.1016/S0040-4020(01)89449-7