N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Base Information

Chemical Name:N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide
CAS No.:286420-46-0
Molecular Formula:C₅₀H₆₃NO₁₀
Molecular Weight:838.051
Hs Code.:

N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Synonyms:N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Chemical Property of N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

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Technology Process of N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

There total 1 articles about N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 116514-50-2,128962-63-0,131545-02-3,136758-06-0,99409-34-4,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 196876-39-8
1-octyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 286420-46-0
N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

Guidance literature:: With tetrabutylammomium bromide; copper(ll) bromide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/S0960-894X(00)00207-9

Reference yield: 79.0%

: 286420-46-0
N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

: 286420-49-3
N-[(2R,3R,4R,5S,6R)-6-Benzyloxymethyl-5-hydroxy-2-octyloxy-4-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With hydrochloric acid diethyl ether; sodium cyanoborohydride; In N,N-dimethyl-formamide; at 0 - 5 ℃; for 3h;
DOI:10.1016/S0960-894X(00)00207-9

Reference yield:

: 286420-46-0
N-[(2R,4aR,6R,7R,8R,8aS)-6-Octyloxy-2-phenyl-8-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

: 286420-52-8
N-[(2R,3R,4R,5S,6R)-6-Benzyloxymethyl-2-octyloxy-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-4-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaBH₃CN; HCl*Et₂O / dimethylformamide / 3 h / 0 - 5 °C

2: BF₃*Et₂O / CH₂Cl₂ / 3 h / -10 - 20 °C

3: NaHCO₃; MeONa / methanol

With boron trifluoride diethyl etherate; sodium methylate; hydrochloric acid diethyl ether; sodium cyanoborohydride; sodium hydrogencarbonate; In methanol; dichloromethane; N,N-dimethyl-formamide; 1: reductive ring opening / 2: glycosylation / 3: Deacetylation;
DOI:10.1016/S0960-894X(00)00207-9