Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

Base Information

Chemical Name:Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine
CAS No.:126568-40-9
Molecular Formula:C₂₂H₂₉NO₅
Molecular Weight:387.476
Hs Code.:

Synonyms:Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

Suppliers and Price of Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

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Technology Process of Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

There total 1 articles about Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99878-63-4
4-O-benzyl-2,3-O-bis(methoxymethyl)-L-threose

: 100-46-9
benzylamine

: 126568-40-9
Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

Guidance literature:: In diethyl ether; at 0 ℃; for 0.25h;
DOI:10.1016/S0040-4039(01)80739-5

Reference yield:

: 126568-40-9
Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

: 60656-87-3
benzyloxyacetoaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / -60 °C

2: concd. HCl / methanol / 1 h / Heating

3: toluene / 2 h / Heating

4: HIO₄ / methanol / 1 h / 0 °C

With hydrogenchloride; periodic acid; In tetrahydrofuran; methanol; toluene;
DOI:10.1016/S0040-4039(01)80739-5

Reference yield:

: 126568-40-9
Benzyl-[(2S,3S)-4-benzyloxy-2,3-bis-methoxymethoxy-but-(E)-ylidene]-amine

: 14231-57-3
(R)-N-benzyl-2-phenylglycinol

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 2 h / -60 °C

2: concd. HCl / methanol / 1 h / Heating

3: toluene / 2 h / Heating

4: HIO₄ / methanol / 1 h / 0 °C

5: NaBH₄ / methanol / 1 h / Ambient temperature

6: CF₃CO₂H / CH₂Cl₂ / 1.5 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; periodic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4039(01)80739-5