1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

Base Information

Chemical Name:1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene
CAS No.:910792-55-1
Molecular Formula:C₁₈H₂₀O₂
Molecular Weight:268.356
Hs Code.:

Synonyms:1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

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Chemical Property of 1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

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Technology Process of 1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

There total 1 articles about 1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 2746-25-0
p-Methoxybenzyl bromide

: 910792-55-1
1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran;

Reference yield: 80.0%

: 910792-55-1
1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

: 4-((4-Methoxybenzyl)oxy)-4-phenylbutan-2-one

Guidance literature:: With Pd((-)-sparteine)2Cl₂; oxygen; In N,N-dimethyl acetamide; water; at 70 ℃; for 24h;
DOI:10.1021/ol061662h

Reference yield:

: 910792-55-1
1-methoxy-4-{[(1-phenylbut-3-enyl)oxy]methyl}benzene

: 67008-23-5
(2R)-2-((2R)-2-hydroxy-2-phenylethyl)-1-methylpiperidine

Guidance literature:: Multi-step reaction with 10 steps

1: aq. NaIO₄; OsO₄ / tetrahydrofuran

2: diethyl ether / -78 °C

3: 82 percent / DPPA; DEAD; PPh₃ / tetrahydrofuran / 12 h / 0 - 20 °C

4: 94 percent / LAH / diethyl ether

5: 85 percent / dioxane

6: 91 percent / KHMDS / tetrahydrofuran; dimethylformamide

7: 94 percent / Grubbs' catalyst / benzene

8: 94 percent / H₂ / PtO₂ / ethyl acetate

9: 75 percent / DDQ; H₂O / CH₂Cl₂ / 0.25 h / 20 °C

10: 78 percent / LAH / tetrahydrofuran / 6 h / Heating

With sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; diphenyl-phosphinic acid; water; hydrogen; potassium hexamethylsilazane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; platinum(IV) oxide; Grubbs catalyst first generation; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene; 1: Oxidative cleavage / 2: Addition / 3: Substitution / 4: Reduction / 5: Acylation / 6: Alkylation / 7: Cyclization / 8: Catalytic hydrogenation / 9: Oxidation / 10: Reduction;