dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

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Chemical Name:dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide
CAS No.:244228-83-9
Molecular Formula:C₂₄H₂₁N₃O
Molecular Weight:367.45
Hs Code.:

Synonyms:dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

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Chemical Property of dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

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Technology Process of dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

There total 3 articles about dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: dicyano(7,7-dimethyl-2,5-di-p-tolyl-3,4-diaza-bicyclo[4.1.0]hepta-2,4-dien-3-ium-3-yl)methanide

: 244228-83-9
dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

Guidance literature:: dicyano(7,7-dimethyl-2,5-di-p-tolyl-3,4-diaza-bicyclo[4.1.0]hepta-2,4-dien-3-ium-3-yl)methanide; With acetic acid; at 80 ℃; for 1h;

With water; In acetic acid; at 80 ℃;
DOI:10.1016/S0040-4020(99)00516-5

Reference yield:

: 7,7-dimethyl-2,5-bis(p-tolyl)-3,4-diazanorcaradiene

: 244228-83-9
dicyano(2,2-dimethyl-3-(4-methyl-benzoyl)-5-p-tolyl-1-aza-cyclopenta-3,5-dien-1-ium-1-yl)methanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 81 percent / ethyl acetate / 3 h / 20 °C

2.1: AcOH / 1 h / 80 °C

2.2: 41 percent / H₂O / acetic acid / 80 °C

With acetic acid; In ethyl acetate; 1.1: Substitution / 2.1: Rearrangement / 2.2: Hydrolysis;
DOI:10.1016/S0040-4020(99)00516-5