dicyclohexylmethanone O-oxiran-2-yl methyl oxime

Base Information

Chemical Name:dicyclohexylmethanone O-oxiran-2-yl methyl oxime
CAS No.:1630039-05-2
Molecular Formula:C₁₆H₂₇NO₂
Molecular Weight:265.396
Hs Code.:

Synonyms:dicyclohexylmethanone O-oxiran-2-yl methyl oxime

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Chemical Property of dicyclohexylmethanone O-oxiran-2-yl methyl oxime

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Technology Process of dicyclohexylmethanone O-oxiran-2-yl methyl oxime

There total 2 articles about dicyclohexylmethanone O-oxiran-2-yl methyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 6316-03-6
dicyclohexyl ketone oxime

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 1630039-05-2
dicyclohexylmethanone O-oxiran-2-yl methyl oxime

Guidance literature:: dicyclohexyl ketone oxime; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

epichlorohydrin; In N,N-dimethyl-formamide; at 20 ℃; for 36.1667h;
DOI:10.3390/molecules19033417

Reference yield:

: 119-60-8
dicyclohexyl ketone

: 1630039-05-2
dicyclohexylmethanone O-oxiran-2-yl methyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride / Alkaline conditions

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 36.17 h / 20 °C

With hydroxylamine hydrochloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.3390/molecules19033417

Reference yield: 63.0%

: 1630039-05-2
dicyclohexylmethanone O-oxiran-2-yl methyl oxime

: 144-62-7,97993-78-7
oxalic acid

: 75-31-0
isopropylamine

: dicyclohexylmethanone O-2-hydroxy-3-(isopropylamino)propyl oxime hydrogen oxalate

Guidance literature:: dicyclohexylmethanone O-oxiran-2-yl methyl oxime; isopropylamine; In toluene; at 120 ℃; for 24h; Sealed tube;

oxalic acid; In diethyl ether; acetone;
DOI:10.3390/molecules19033417