pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

Base Information

Chemical Name:pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide
CAS No.:1217308-99-0
Molecular Formula:C₄₄H₂₅Cl₁₂NO₅
Molecular Weight:1073.12
Hs Code.:

Synonyms:pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

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Chemical Property of pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

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Technology Process of pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

There total 1 articles about pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.5%

: 1217308-98-9
bis[2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl]-[4-(2-aminoethyl)-2,3,5,6-tetrachlorophenyl]methane

: 204705-13-5
1-pyrenecarboxylic acid N-hydroxysuccinimide ester

: 1217308-99-0
pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 50 ℃; for 2h;
DOI:10.1016/j.bmc.2009.11.034

Reference yield: 99.0%

: 1217308-99-0
pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide

: 1217309-00-6
bis(2,3,5,6-tetrachlorophenyl)-{4-[2-(1-pyrenecarbonyl)aminoethyl]-2,3,5,6-tetrachlorophenyl} methyl radical

Guidance literature:: pyrene-1-carboxylic acid (2-{4-[bis-(2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl)-methyl]-2,3,5,6-tetrachloro-phenyl}-ethyl)-amide; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; at 20 ℃;

With chloranil; In tetrahydrofuran; for 1h;
DOI:10.1016/j.bmc.2009.11.034