4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

Base Information

Chemical Name:4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone
CAS No.:1467100-92-0
Molecular Formula:C₁₈H₂₂O₄
Molecular Weight:302.37
Hs Code.:

Synonyms:4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

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Technology Process of 4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

There total 3 articles about 4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 950772-87-9
4-(prop-2-yn-1-yloxy)cyclohexanone

: 1467100-92-0
4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

Guidance literature:: With pyridine; copper diacetate; at 55 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.08.080

Reference yield:

: 1447817-83-5
4-(prop-2-yn-1-yloxy)cyclohexan-1-ol

: 1467100-92-0
4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 24 h / 20 °C

2: pyridine; copper diacetate / 55 °C / Inert atmosphere

With pyridine; copper diacetate; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/j.tetlet.2013.08.080

Reference yield:

: 556-48-9
1,4-Cyclohexanediol

: 1467100-92-0
4,4'-[hexa-2,4-diyn-1,6-diylbis(oxy)]dicyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 24 h / 0 °C / Schlenk technique; Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 24 h / 20 °C

3: pyridine; copper diacetate / 55 °C / Inert atmosphere

With pyridine; copper diacetate; sodium hydride; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.08.080