(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

Base Information

Chemical Name:(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid
CAS No.:1562193-33-2
Molecular Formula:C₁₉H₂₀N₂O₆S
Molecular Weight:404.444
Hs Code.:

Synonyms:(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

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Chemical Property of (R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

Chemical Property:

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Technology Process of (R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

There total 1 articles about (R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92613-96-2
(R)-2-(benzyloxycarbonylamino)-3-mercapto-3-methylbutanoic acid

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1562193-33-2
(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

Guidance literature:: (R)-2-(benzyloxycarbonylamino)-3-mercapto-3-methylbutanoic acid; With sodium hydrogencarbonate; In ethanol; water; for 0.333333h;

ortho-nitrofluorobenzene; In ethanol; water; for 6h; Reflux;

Reference yield:

: 1562193-33-2
(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

: 1562193-37-6
(R)-3-(2-aminophenylthio)-2-(benzyloxycarbonylamino)-3-methylbutanoic acid

Guidance literature:: With methanol; ammonium chloride; zinc; for 6h; Reflux;

Reference yield:

: 1562193-33-2
(R)-2-(benzyloxycarbonylamino)-3-methyl-3-(2-nitrophenylthio)butanoic acid

: 1562193-39-8
(R)-benzyl 2,2-dimethyl-4-oxo-2,3,4,5-tetrahydrobenzo[b][1,4]thiazepin-3-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; zinc; ammonium chloride / 6 h / Reflux

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 - 80 °C

With methanol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; N-ethyl-N,N-diisopropylamine; zinc; In N,N-dimethyl-formamide;