5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

Base Information

Chemical Name:5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine
CAS No.:1290632-18-6
Molecular Formula:C₁₆H₁₉N₇O₅S₂
Molecular Weight:453.503
Hs Code.:

Synonyms:5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

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Chemical Property of 5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

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Technology Process of 5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

There total 5 articles about 5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1290632-15-3
5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-1,3,4-thiadiazol-2-amine

: 1290632-18-6
5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 0.5h;
DOI:10.1016/j.carres.2011.01.010

Reference yield:

: 13980-76-2
1-(4-methoxyphenyl)-1H-tetrazole-5-thiol

: 1290632-18-6
5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide

2: hydrazine hydrate / ethanol / 4 h / Reflux

3: benzene / 4 h / Reflux

4: phosphoric acid; acetic anhydride / 24 h / 20 °C

5: methanol; sodium methylate / 0.5 h / 20 °C

With methanol; phosphoric acid; sodium methylate; acetic anhydride; hydrazine hydrate; sodium hydroxide; In ethanol; benzene;
DOI:10.1016/j.carres.2011.01.010

Reference yield:

: 13980-79-5
[1-(4-methoxy-phenyl)-1H-tetrazol-5-ylsulfanyl]-acetic acid ethyl ester

: 1290632-18-6
5-(1-(4-methoxyphenyl)-1H-tetrazol-5-ylsulfanylmethyl)-N-β-D-xylopyranosyl-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / ethanol / 4 h / Reflux

2: benzene / 4 h / Reflux

3: phosphoric acid; acetic anhydride / 24 h / 20 °C

4: methanol; sodium methylate / 0.5 h / 20 °C

With methanol; phosphoric acid; sodium methylate; acetic anhydride; hydrazine hydrate; In ethanol; benzene;
DOI:10.1016/j.carres.2011.01.010