2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

Base Information

Chemical Name:2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol
CAS No.:1383540-90-6
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

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Chemical Property of 2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

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Technology Process of 2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

There total 6 articles about 2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

: 1204357-73-2
2-methoxy-5-(6,7,8-trimethoxy-3,4-dihydroisoquinolin-1-yl)phenol

: 1383540-90-6
2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 2h; Reflux;
DOI:10.1002/ardp.201100169

Reference yield:

: C₂₁H₂₅NO₇

: 1383540-90-6
2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / acetonitrile / 4 h / Reflux

2: sodium hydroxide / ethanol; water / 2 h / 20 °C

3: sodium tetrahydroborate / methanol / 2 h / Reflux

With sodium tetrahydroborate; sodium hydroxide; trichlorophosphate; In methanol; ethanol; water; acetonitrile;
DOI:10.1002/ardp.201100169

Reference yield:

: C₂₁H₂₃NO₆

: 1383540-90-6
2-methoxy-5-(6,7,8-trimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol; water / 2 h / 20 °C

2: sodium tetrahydroborate / methanol / 2 h / Reflux

With sodium tetrahydroborate; sodium hydroxide; In methanol; ethanol; water;
DOI:10.1002/ardp.201100169