Technology Process of C57H77N5O11
There total 3 articles about C57H77N5O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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284666-64-4
1,6,17,29-tetrakis(benzyloxy)-7,10,18,21-tetraoxo-6,11,17,22,28-pentaazaoctacosane
- Guidance literature:
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Multi-step reaction with 2 steps
1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen; lithium hydroxide / methanol / Inert atmosphere
With
dmap; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
methanol; dichloromethane;
DOI:10.1021/ol301869x
DOI:10.1021/ol301869x
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284666-57-5
28-(tert-butoxycarbonyl)-1,6,17,29-tetrakis(benzyloxy)-7,10,18,21-tetraoxo-6,11,17,22,28-pentaazaoctacosane
- Guidance literature:
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Multi-step reaction with 3 steps
1: trifluoroacetic acid; sodium hydrogencarbonate / dichloromethane / Inert atmosphere
2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 20 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen; lithium hydroxide / methanol / Inert atmosphere
With
dmap; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
methanol; dichloromethane;
DOI:10.1021/ol301869x
DOI:10.1021/ol301869x