Technology Process of C27H37FO3S
There total 6 articles about C27H37FO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 ℃;
for 2h;
Overall yield = 1.53 g;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium; ammonia; tert-butyl alcohol / tetrahydrofuran / 1.5 h / -50 °C
2.1: iodine / 12 h / 60 °C
3.1: potassium tert-butylate / tetrahydrofuran / 3 h / 0 - 60 °C
3.2: 2 h / 60 °C
4.1: hydrogenchloride; water / tetrahydrofuran / 12 h / 20 °C
5.1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 2 h / -78 °C
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium tert-butylate; ammonia; water; iodine; lithium; lithium hexamethyldisilazane; tert-butyl alcohol;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: iodine / 12 h / 60 °C
2.1: potassium tert-butylate / tetrahydrofuran / 3 h / 0 - 60 °C
2.2: 2 h / 60 °C
3.1: hydrogenchloride; water / tetrahydrofuran / 12 h / 20 °C
4.1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / 2 h / -78 °C
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium tert-butylate; water; iodine; lithium hexamethyldisilazane;
In
tetrahydrofuran;
