4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

Base Information

Chemical Name:4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole
CAS No.:94418-11-8
Molecular Formula:C₂₉H₂₄ClN₃O₅S
Molecular Weight:562.046
Hs Code.:

Synonyms:4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

Chemical Property:

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Technology Process of 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

There total 5 articles about 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 94418-09-4
4-<(Z)-1-Carboxy-1-trityloxyimino>methyl-2-chloroacetamidothiazole

: 78-95-5
chloroacetone

: 94418-11-8
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; overnight;
DOI:10.1002/jhet.5570210435

Reference yield:

: 76-83-5
trityl chloride

: 94418-11-8
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / Triethylamine / dimethylformamide / 24 h

2: 94 percent / 35percent aq. NaOH / ethanol / 3 h / 25 °C

3: 82 percent / Triethylamine / dimethylformamide / overnight

With sodium hydroxide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210435

Reference yield:

: 94418-08-3
4-<(Z)-1-Carbethoxy-1-hydroxyimino>methyl-2-chloroacetamidothiazole

: 94418-11-8
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / Triethylamine / dimethylformamide / 24 h

2: 94 percent / 35percent aq. NaOH / ethanol / 3 h / 25 °C

3: 82 percent / Triethylamine / dimethylformamide / overnight

With sodium hydroxide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210435