2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

Base Information

Chemical Name:2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide
CAS No.:765951-41-5
Molecular Formula:C₁₄H₁₅N₃O₃S
Molecular Weight:305.357
Hs Code.:

Synonyms:2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

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Chemical Property of 2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

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Technology Process of 2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

There total 1 articles about 2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 33603-90-6
(2Z)-2-bromo-3-phenyl-2-propenal

: 155603-86-4
1-(N,N-dimethylsulfamoyl)-2-(tributylstannyl)imidazole

: 765951-41-5
2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

Guidance literature:: With silver(l) oxide; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 100 ℃; for 48h;
DOI:10.1002/hlca.200590050

Reference yield: 82.0%

: 765951-41-5
2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

: 855780-55-1
2-[(1RS)-1-benzyl-2-hydroxyethyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

Guidance literature:: With tri-n-butyl-tin hydride; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 20 ℃; for 14h;
DOI:10.1002/hlca.200590050

Reference yield:

: 765951-41-5
2-[(E)-1-formyl-2-phenylethenyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

: 855780-71-1
5-benzyl-2-[(1RS)-1-benzyl-2-hydroxyethyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 82 percent / Bu₃SnH; AcOH / [Pd(PPh₃)4] / benzene / 14 h / 20 °C

2.1: 79 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 16 h / 20 °C

3.1: s-BuLi / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

3.2: 67 percent / tetrahydrofuran; cyclohexane / 3 h / -78 - 20 °C

4.1: 81 percent / Bu₄NF / tetrahydrofuran / 2.5 h / 20 °C

With dmap; tetrabutyl ammonium fluoride; sec.-butyllithium; tri-n-butyl-tin hydride; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; cyclohexane; benzene;
DOI:10.1002/hlca.200590050