(3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

Base Information

Chemical Name:(3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol
CAS No.:1214270-95-7
Molecular Formula:C₃₂H₃₉NO₄
Molecular Weight:501.666
Hs Code.:

Synonyms:(3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

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Chemical Property of (3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

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Technology Process of (3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

There total 3 articles about (3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1214270-92-4
(1E,4S)-4-[(4-methoxybenzyl)oxy]-pent-1-en-1-yl phenyl sulfone

: 6783-05-7
trans-2-phenylvinylboronic acid

: 97682-96-7,99726-01-9,127505-65-1
(2S)-1-(phenylmethoxy)but-3-en-2-ylamine

: 1214270-95-7
(3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

: (3R,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-1-phenylhept-1-en-4-ol

Guidance literature:: (1E,4S)-4-[(4-methoxybenzyl)oxy]-pent-1-en-1-yl phenyl sulfone; With potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 20 ℃; for 24h; Sonication;

trans-2-phenylvinylboronic acid; (2S)-1-(phenylmethoxy)but-3-en-2-ylamine; In dichloromethane; at 20 ℃; for 48h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/b918233k

Reference yield:

: 4-(4-methoxybenzyloxy)pentane-1,2-diol

: 1214270-95-7
(3S,4R,6S,E)-3-((S)-1-(benzyloxy)but-3-en-2-ylamino)-6-(4-methoxybenzyloxy)-4-methoxy-1-phenylhept-1-en-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; potassium bromide; sodium hydrogencarbonate / water; dichloromethane / 0.5 h / 0 °C

2: dichloromethane / 48 h / 32 °C / Inert atmosphere

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In dichloromethane; water; 2: |Petasis Reaction;
DOI:10.1021/jo5005923