5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine

Base Information

• Chemical Name: 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine
• CAS No.: 929902-03-4
• Molecular Formula: C₂₆H₃₈N₂O₇Si
• Molecular Weight: 518.682

Synonyms:5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine

Chemical Property of 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine

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Technology Process of 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine

There total 2 articles about 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

5'-O-(t-butyldimethylsilyl)-2',3'-O-isopropylideneuridine (102147-76-2) + p-methoxybenzyl chloride (824-94-2) → 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N3-(p-methoxybenzyl)uridine (929902-03-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1055/s-2006-956464

Reference yield: 60.0%

C32H42N2O7SeSi → C26H38N2O7Si + 5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N3-(p-methoxybenzyl)uridine (929902-03-4) + C26H38N2O7Si

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; In toluene; for 6h; Heating;

DOI:10.1055/s-2006-956464

Reference yield: 92.0%

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N3-(p-methoxybenzyl)uridine (929902-03-4) + diphenyl diselenide (1666-13-3) → C32H42N2O7SeSi

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -80 ℃;

DOI:10.1055/s-2006-956464

upstream raw materials:

5'-O-(t-butyldimethylsilyl)-2',3'-O-isopropylideneuridine

p-methoxybenzyl chloride

Downstream raw materials:

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-6-iodo-N₃-(p-methoxybenzyl)uridine

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)-6-phenyluridine

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-N₃-(p-methoxybenzyl)-6-(p-nitrophenyl)uridine

5'-O-tert-butyldimethylsilyl-2',3'-O-isopropylidene-6-(n-butyl)-N₃-(p-methoxybenzyl)uridine

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