2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

Base Information

Chemical Name:2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd
CAS No.:154853-68-6
Molecular Formula:C₁₁H₅F₇O₃
Molecular Weight:318.148
Hs Code.:

Synonyms:2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

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Chemical Property of 2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

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Technology Process of 2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

There total 4 articles about 2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 154853-71-1
2-Methoxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

: 154853-68-6
2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

Guidance literature:: With boron tribromide; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 118745-68-9
4-bromo-2,6-di(hydroxymethyl)anisole diacacetate

: 154853-68-6
2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Cu-bronze / dimethylformamide / 140 - 150 °C

2: 90 percent / 5M KOH / ethanol / 5 h / Ambient temperature

3: 53 percent / Na₂Cr₂O₇*2H₂O, H₂SO₄ / H₂O / 3.5 h / 50 °C

4: 94 percent / BBr₃ / CH₂Cl₂ / 1 h / Ambient temperature

With potassium hydroxide; sodium dichromate; sulfuric acid; boron tribromide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 154853-70-0
2,6-Bis(hydroxymethyl)-4-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>anisol

: 154853-68-6
2-Hydroxy-5-<1,2,2,2-tetrafluor-1-(trifluormethyl)ethyl>benzol-1,3-dicarbaldehyd

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / Na₂Cr₂O₇*2H₂O, H₂SO₄ / H₂O / 3.5 h / 50 °C

2: 94 percent / BBr₃ / CH₂Cl₂ / 1 h / Ambient temperature

With sodium dichromate; sulfuric acid; boron tribromide; In dichloromethane; water;