N-benzyl-N-prop-2-ynylcarbamoyl chloride

Base Information

Chemical Name:N-benzyl-N-prop-2-ynylcarbamoyl chloride
CAS No.:878277-25-9
Molecular Formula:C₁₁H₁₀ClNO
Molecular Weight:207.659
Hs Code.:

Synonyms:N-benzyl-N-prop-2-ynylcarbamoyl chloride

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Chemical Property of N-benzyl-N-prop-2-ynylcarbamoyl chloride

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Technology Process of N-benzyl-N-prop-2-ynylcarbamoyl chloride

There total 1 articles about N-benzyl-N-prop-2-ynylcarbamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1197-51-9
N-propargylbenzylamine

: 116-16-5
1,1,1,3,3,3-hexachloro-propan-2-one

: 878277-25-9
N-benzyl-N-prop-2-ynylcarbamoyl chloride

Guidance literature:: With pyridine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/ja052175k

Reference yield: 29.0%

: 878277-25-9
N-benzyl-N-prop-2-ynylcarbamoyl chloride

: 591-51-5
phenyllithium

: 861956-76-5
Se-phenyl N-benzyl-N-(prop-2-ynyl)carbamoselenoate

Guidance literature:: phenyllithium; With selenium; In tetrahydrofuran; diethyl ether; cyclohexane; at 0 ℃; for 0.0833333h;

N-benzyl-N-prop-2-ynylcarbamoyl chloride; In tetrahydrofuran; diethyl ether; cyclohexane; at 0 - 20 ℃;
DOI:10.1021/ja052175k

Reference yield:

: 878277-25-9
N-benzyl-N-prop-2-ynylcarbamoyl chloride

: (Z)-1-benzyl-3-phenylselenomethyleneazetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: Se / tetrahydrofuran; diethyl ether; cyclohexane / 0.08 h / 0 °C

1.2: 29 percent / tetrahydrofuran; diethyl ether; cyclohexane / 0 - 20 °C

2.1: 59 percent / Pd(PPh₃)4 / toluene / 1 h / Heating

With selenium; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; cyclohexane; toluene;
DOI:10.1021/ja052175k