4-Methylbenzaldehyde N-phenylthiosemicarbazone

Base Information

Chemical Name:4-Methylbenzaldehyde N-phenylthiosemicarbazone
CAS No.:74959-63-0
Molecular Formula:C₁₅H₁₅N₃S
Molecular Weight:269.37
Hs Code.:
European Community (EC) Number:657-239-4
ChEMBL ID:CHEMBL254121

Synonyms:CHEMBL254121;SALOR-INT L463264-1EA;AKOS003416499;1-phenyl-3-[(E)-p-tolylmethyleneamino]thiourea;4-methylbenzaldehyde 4-phenyl-3-thiosemicarbazone;4-METHYLBENZALDEHYDE N-PHENYLTHIOSEMICARBAZONE;(e)-2-(4-methylbenzylidene)-N-phenylhydrazine-1-carbothioamide

Suppliers and Price of 4-Methylbenzaldehyde N-phenylthiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-METHYLBENZALDEHYDE-N-PHENYLTHIOSEMICARBAZONE 95.00%
5MG
$ 495.43

Total 1 raw suppliers

Chemical Property of 4-Methylbenzaldehyde N-phenylthiosemicarbazone

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:269.09866866
Heavy Atom Count:19
Complexity:303

Purity/Quality:

97% ^*data from raw suppliers

4-METHYLBENZALDEHYDE-N-PHENYLTHIOSEMICARBAZONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C=NNC(=S)NC2=CC=CC=C2
Isomeric SMILES:CC1=CC=C(C=C1)/C=N/NC(=S)NC2=CC=CC=C2

Technology Process of 4-Methylbenzaldehyde N-phenylthiosemicarbazone

There total 6 articles about 4-Methylbenzaldehyde N-phenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 83639-13-8,34025-63-3
2,4-bis(4-methylphenyl)-3-azabicyclo[3.3.1]nonan-9-one

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: C₂₉H₃₂N₄S

: 74959-63-0
4-methylbenzaldehyde-4-phenylthiosemicarbazone

Guidance literature:: In ethanol; chloroform; at 90 - 100 ℃; for 96h; Acidic conditions;
DOI:10.3109/14756366.2010.525508

Reference yield: 80.0%

: 104-87-0
4-methyl-benzaldehyde

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 74959-63-0
4-methylbenzaldehyde-4-phenylthiosemicarbazone

Guidance literature:: In ethanol; ethylbenzene; for 4.5h; Reflux;
DOI:10.2174/1570178614666161123145054

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 74959-63-0
4-methylbenzaldehyde-4-phenylthiosemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 1 h

2: methanol / 6 h / Reflux

With hydrazine hydrate; In methanol;
DOI:10.1039/d1ob01521d