1,3-bismethyl>benzene

Base Information

Chemical Name:1,3-bismethyl>benzene
CAS No.:102586-94-7
Molecular Formula:C₄₈H₆₂N₄O₈
Molecular Weight:823.042
Hs Code.:

1,3-bis<bis<5-(ethoxycarbonyl)-4-ethyl-3-methyl-2-pyrryl>methyl>benzene

Synonyms:1,3-bismethyl>benzene

Suppliers and Price of 1,3-bismethyl>benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-bismethyl>benzene

Chemical Property:

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Technology Process of 1,3-bismethyl>benzene

There total 3 articles about 1,3-bismethyl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 4949-58-0
2-(ethyloxycarbonyl)-3-ethyl-4-methylpyrrole

: 626-19-7
Isophthalaldehyde

: 102586-94-7
1,3-bismethyl>benzene

Guidance literature:: With hydrogenchloride; In ethanol; for 10h; Heating;
DOI:10.1021/ja00181a038

Reference yield:

: 100780-37-8
2-nitro-3-acetoxy-pentane

: 102586-94-7
1,3-bismethyl>benzene

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / tetrahydrofuran; propan-2-ol / 4 h / Ambient temperature

2: 93 percent / concd. HCl / ethanol / 10 h / Heating

With hydrogenchloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; ethanol; isopropyl alcohol;
DOI:10.1021/ja00181a038

Reference yield:

: 20575-40-0,138668-19-6,138668-26-5
2-nitropentan-3-ol

: 102586-94-7
1,3-bismethyl>benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / concd. H₂SO₄ / 1 h

2: DBU / tetrahydrofuran; propan-2-ol / 4 h / Ambient temperature

3: 93 percent / concd. HCl / ethanol / 10 h / Heating

With hydrogenchloride; sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; ethanol; isopropyl alcohol;
DOI:10.1021/ja00181a038