C₃₄H₅₃NO₃S₅Si

Base Information

Chemical Name:C₃₄H₅₃NO₃S₅Si
CAS No.:1311280-67-7
Molecular Formula:C₃₄H₅₃NO₃S₅Si
Molecular Weight:712.215
Hs Code.:

C<sub>34</sub>H<sub>53</sub>NO<sub>3</sub>S<sub>5</sub>Si

Synonyms:C₃₄H₅₃NO₃S₅Si

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Chemical Property of C₃₄H₅₃NO₃S₅Si

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Technology Process of C₃₄H₅₃NO₃S₅Si

There total 1 articles about C₃₄H₅₃NO₃S₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 6007-26-7
2-methyl-1,3-dithian

: C₁₃H₂₆OS₂Si

: 71535-50-7,77210-52-7,62596-64-9
(S)-(+)-2-benzyl-1-(p-tolylsulfonyl)aziridine

: 1311280-67-7
C₃₄H₅₃NO₃S₅Si

Guidance literature:: 2-methyl-1,3-dithian; With potassium tert-butylate; tert.-butyl lithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₁₃H₂₆OS₂Si; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(S)-(+)-2-benzyl-1-(p-tolylsulfonyl)aziridine; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol2010598

Reference yield: 88.0%

: 1311280-67-7
C₃₄H₅₃NO₃S₅Si

: 1311280-55-3
C₂₈H₃₉NO₃S₅

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol2010598

Reference yield:

: 1311280-67-7
C₃₄H₅₃NO₃S₅Si

: C₂₂H₂₇NO₄S

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / methanol; water / 12 h / 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

4: N-chloro-succinimide; silver nitrate / water; acetonitrile / 0.08 h / 0 °C / Inert atmosphere

5: lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere

With hydrogenchloride; N-chloro-succinimide; lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride; sodium hydride; silver nitrate; triethylamine; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1021/ol2010598