N-methyl-N--2-phenylglycine

Base Information

Chemical Name:N-methyl-N--2-phenylglycine
CAS No.:81278-21-9
Molecular Formula:C₂₁H₂₃NO₄
Molecular Weight:353.418
Hs Code.:

N-methyl-N-<p-methoxy-o-(3-butenyl)benzoyl>-2-phenylglycine

Synonyms:N-methyl-N--2-phenylglycine

Suppliers and Price of N-methyl-N--2-phenylglycine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N--2-phenylglycine

Chemical Property:

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Technology Process of N-methyl-N--2-phenylglycine

There total 4 articles about N-methyl-N--2-phenylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 81278-22-0
N-methyl-N--2-phenylglycine ethyl ester

: 81278-21-9
N-methyl-N--2-phenylglycine

Guidance literature:: With sodium hydroxide; In ethanol; for 0.5h; Heating;
DOI:10.1021/jo00133a041

Reference yield:

: 81278-31-1
N-methyl-2-phenylglycine ethyl ester

: 81278-21-9
N-methyl-N--2-phenylglycine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, N,N-dimethylformamide, 2.) triethylamine / 1.) ether, 5 deg C, 19 h, 2.) benzene, 25 deg C, 8 h

2: 94 percent / aq. sodium hydroxide / ethanol / 0.5 h / Heating

With sodium hydroxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In ethanol;
DOI:10.1021/jo00133a041

Reference yield:

: 81278-32-2
p-methoxy-o-(3-butenyl)benzoic acid

: 81278-21-9
N-methyl-N--2-phenylglycine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, N,N-dimethylformamide, 2.) triethylamine / 1.) ether, 5 deg C, 19 h, 2.) benzene, 25 deg C, 8 h

2: 94 percent / aq. sodium hydroxide / ethanol / 0.5 h / Heating

With sodium hydroxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In ethanol;
DOI:10.1021/jo00133a041