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C19H36O2Si

Base Information Edit
C<sub>19</sub>H<sub>36</sub>O<sub>2</sub>Si

Synonyms:C19H36O2Si

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Chemical Property of C19H36O2Si Edit
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Technology Process of C19H36O2Si

There total 11 articles about C19H36O2Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 ℃; for 1.5h; pH=7; aq. phosphate buffer;
DOI:10.1016/j.tetlet.2011.10.151
Guidance literature:
Multi-step reaction with 6 steps
1.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C
2.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 6 h / -40 °C
3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / 4 h / 40 °C
3.2: 12 h / -78 - 0 °C
4.1: 2,6-dimethylpyridine / dichloromethane / 0.17 h / 20 °C
5.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / water; acetonitrile / 1.5 h / 80 °C
6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 0 °C / pH 7 / aq. phosphate buffer
With 2,6-dimethylpyridine; borane-THF; palladium diacetate; Dess-Martin periodane; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; tris-(o-tolyl)phosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; water; acetonitrile; 5.1: Heck reaction;
DOI:10.1016/j.tetlet.2011.10.151
Guidance literature:
Multi-step reaction with 9 steps
1.1: mercury(II) diacetate / 36 h / Reflux
2.1: methylaluminium bis(4-bromo-2,6-di-tert.-butylphenoxide) / dichloromethane / 0.25 h / -78 °C
3.1: n-butyllithium / tetrahydrofuran
3.2: 2 h / -78 °C
4.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C
5.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 6 h / -40 °C
6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / 4 h / 40 °C
6.2: 12 h / -78 - 0 °C
7.1: 2,6-dimethylpyridine / dichloromethane / 0.17 h / 20 °C
8.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / water; acetonitrile / 1.5 h / 80 °C
9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 0 °C / pH 7 / aq. phosphate buffer
With 2,6-dimethylpyridine; n-butyllithium; borane-THF; mercury(II) diacetate; palladium diacetate; Dess-Martin periodane; methylaluminium bis(4-bromo-2,6-di-tert.-butylphenoxide); triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; tris-(o-tolyl)phosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; water; acetonitrile; 2.1: Claisen rearrangement / 8.1: Heck reaction;
DOI:10.1016/j.tetlet.2011.10.151
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