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Technology Process of C58H99IO7Si4

C58H99IO7Si4

Base Information
  • Chemical Name:C58H99IO7Si4
  • CAS No.:1163245-59-7
  • Molecular Formula:C58H99IO7Si4
  • Molecular Weight:1147.67
  • Hs Code.:
C<sub>58</sub>H<sub>99</sub>IO<sub>7</sub>Si<sub>4</sub>

Synonyms:C58H99IO7Si4

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Chemical Property of C58H99IO7Si4
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Technology Process of C58H99IO7Si4

There total 1 articles about C58H99IO7Si4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C<sub>52</sub>H<sub>85</sub>IO<sub>7</sub>Si<sub>3</sub>
1163245-58-6

C52H85IO7Si3

Dimethyl(t-butyl)silyl trifluoromethanesulphonate

Dimethyl(t-butyl)silyl trifluoromethanesulphonate

C<sub>58</sub>H<sub>99</sub>IO<sub>7</sub>Si<sub>4</sub>
1163245-59-7

C58H99IO7Si4

Guidance literature:
With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200802067

Reference yield: 87.0%

C<sub>58</sub>H<sub>99</sub>IO<sub>7</sub>Si<sub>4</sub>
1163245-59-7

C58H99IO7Si4

tert-Butyl-dimethyl-[(2S,3S)-3-((R)-2-methyl-pent-4-ynyl)-oxiranylmethoxy]-silane
309241-57-4

tert-Butyl-dimethyl-[(2S,3S)-3-((R)-2-methyl-pent-4-ynyl)-oxiranylmethoxy]-silane

C<sub>67</sub>H<sub>114</sub>O<sub>9</sub>Si<sub>4</sub>
1163245-60-0

C67H114O9Si4

Guidance literature:
tert-Butyl-dimethyl-[(2S,3S)-3-((R)-2-methyl-pent-4-ynyl)-oxiranylmethoxy]-silane; With tetrakis(triphenylphosphine) palladium(0); trimethylsilyltributyltin; In 1,2-dimethoxyethane; at 100 ℃; Inert atmosphere;
With tetrabutyl ammonium fluoride; In tetrahydrofuran; dimethyl sulfoxide; at 80 ℃; for 0.75h;
C58H99IO7Si4; With tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In N,N-dimethyl-formamide; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.200802067
upstream raw materials:

C52H85IO7Si3

Downstream raw materials:

C67H114O9Si4

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