2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Base Information

Chemical Name:2,3-dibromo-N,N-diethyl-3-phenylpropanamide
CAS No.:6628-47-3
Molecular Formula:C13H17 Br2 N O
Molecular Weight:363.0882
Hs Code.:

Synonyms:Hydrocinnamamide,a,b-dibromo-N,N-diethyl- (7CI);2,3-Dibromo-N,N-diethyl-3-phenylpropanamide; NSC 60612

Suppliers and Price of 2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Chemical Property:

Vapor Pressure:7E-06mmHg at 25°C
Boiling Point:376.9°Cat760mmHg
Flash Point:181.8°C
Density:1.534g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-dibromo-N,N-diethyl-3-phenylpropanamide

There total 5 articles about 2,3-dibromo-N,N-diethyl-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27829-46-5,84039-69-0,3680-04-4
N,N-diethylcinnamide

: 6628-47-3
(trans)-2,3-dibromo-N,N-diethyl-3-phenylpropanamide

: 2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Guidance literature:: With N-Bromosuccinimide; dimanganese decacarbonyl; In 1,2-dichloro-ethane; at 110 ℃; for 12h; Overall yield = 88 percent; Schlenk technique;
DOI:10.1039/d1cc04534b

Reference yield:

: 27829-46-5
(E)-N,N-diethyl-3-phenylacrylamide

: 6628-47-3
(trans)-2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Guidance literature:: With tetrachloromethane; bromine;
DOI:10.1021/ja01222a007

Reference yield:

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 6628-47-3
(trans)-2,3-dibromo-N,N-diethyl-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: tetrachloromethane; bromine

With tetrachloromethane; bromine; benzene;
DOI:10.1021/ja01222a007