Technology Process of 3,6-bis(N,N-dimethylamino)-9-(3-(N,N-dimethylamino)phenyl)selenoxanthylium bromide
There total 1 articles about 3,6-bis(N,N-dimethylamino)-9-(3-(N,N-dimethylamino)phenyl)selenoxanthylium bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-bromo-N,N-dimethylaniline;
With
magnesium;
In
tetrahydrofuran;
for 1h;
Inert atmosphere;
Reflux;
2,7-bis-N,N-dimethylamino-9H-selenoxanthen-9-one;
In
tetrahydrofuran;
for 4h;
Inert atmosphere;
Reflux;
With
hydrogen bromide;
In
tetrahydrofuran; water; acetic acid;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jm900253g