1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide]

Base Information

• Chemical Name: 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide]
• CAS No.: 252334-27-3
• Molecular Formula: C₄₁H₃₀F₂₀N₈O₂
• Molecular Weight: 1046.71
• Mol file: 252334-27-3.mol

Synonyms:1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide]

Chemical Property of 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide]

There total 2 articles about 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-pyrazoledicarboxylic acid (3112-31-0) → 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide] (252334-27-3)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: Et₃N / tetrahydrofuran

With thionyl chloride; triethylamine; In tetrahydrofuran; 1: Substitution / 2: Acylation;

DOI:10.1515/znb-1999-1012

Reference yield:

1H-pyrazole-3,5-dicarbonyl dichloride (74621-40-2) + N-(2,3,4,5,6-pentafluoro-phenyl)-N'-(3-pentafluorophenylamino-propyl)-propane-1,3-diamine → 1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide] (252334-27-3)

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.1515/znb-1999-1012

Reference yield: 94.0%

1H-pyrazole-3,5-dicarboxylic acid bis-[bis-(3-pentafluorophenylamino-propyl)-amide] (252334-27-3) → N-[5-({bis-[3-(2,4,6-trifluoro-phenylamino)-propyl]-amino}-methyl)-1H-pyrazol-3-ylmethyl]-N'-(2,4,6-trifluoro-phenyl)-N-[3-(2,4,6-trifluoro-phenylamino)-propyl]-propane-1,3-diamine

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Heating;

DOI:10.1515/znb-1999-1012

upstream raw materials:

1H-pyrazole-3,5-dicarbonyl dichloride

3,5-pyrazoledicarboxylic acid