[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

Base Information

Chemical Name:[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt
CAS No.:1000611-51-7
Molecular Formula:C₂₂H₂₅N₃O₅S₂*H₃N
Molecular Weight:492.62
Hs Code.:

Synonyms:[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

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Chemical Property of [1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

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Technology Process of [1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

There total 6 articles about [1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₅N₃O₂S

: 1000611-51-7
[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

Guidance literature:: C₂₂H₂₅N₃O₂S; With pyridine-SO₃ complex; In pyridine; at 20 ℃; for 0.0833333h;

With ammonium hydroxide; In pyridine; water;

Reference yield:

: 1000611-88-0
[2-(4-nitrophenyl)-1-(S)-(4-phenylthiazol-2-yl)ethyl]-carbamic acid tert-butyl ester

: 1000611-51-7
[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 12 h

2: pyridine; sulfur trioxide pyridine complex / 0.08 h / 20 °C

With pyridine; hydrogen; sulfur trioxide pyridine complex; palladium 10% on activated carbon; In methanol;

Reference yield:

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 1000611-51-7
[1-(S)-(phenylthiazol-2-yl)-2-(4-sulfoaminophenyl)ethyl]carbamic acid tert-butyl ester ammonium salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: Lawessons reagent / tetrahydrofuran / 3 h / 20 °C

3.1: acetonitrile / 1.5 h / Reflux

3.2: 2 h

4.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h

5.1: pyridine; sulfur trioxide pyridine complex / 0.08 h / 20 °C

With Lawessons reagent; 4-methyl-morpholine; pyridine; hydrogen; sulfur trioxide pyridine complex; isobutyl chloroformate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;