C₁₃H₁₅NO₂Se

Base Information

• Chemical Name: C₁₃H₁₅NO₂Se
• CAS No.: 1258863-51-2
• Molecular Formula: C₁₃H₁₅NO₂Se
• Molecular Weight: 296.228
• Mol file: 1258863-51-2.mol

Synonyms:C₁₃H₁₅NO₂Se

Chemical Property of C₁₃H₁₅NO₂Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₅NO₂Se

There total 4 articles about C₁₃H₁₅NO₂Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(S)-2-Isocyano-3-methyl-butyric acid benzyl ester (799779-66-1) → C13H15NO2Se (1258863-51-2)

Guidance literature:

With selenium; triethylamine; In tetrahydrofuran; for 1h; Reflux;

DOI:10.1002/psc.1276

Reference yield:

N-formyl-L-valine (4289-97-8) → C13H15NO2Se (1258863-51-2)

Guidance literature:

Multi-step reaction with 3 steps

1: p-toluenesulfonyl chloride / toluene / Reflux

2: Burgess Reagent / dichloromethane / 1.5 h / 50 °C

3: selenium; triethylamine / tetrahydrofuran / 1 h / Reflux

With selenium; Burgess Reagent; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane; toluene;

DOI:10.1002/psc.1276

Reference yield:

N-Formyl-L-valine benzyl ester (71738-67-5) → C13H15NO2Se (1258863-51-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Burgess Reagent / dichloromethane / 1.5 h / 50 °C

2: selenium; triethylamine / tetrahydrofuran / 1 h / Reflux

With selenium; Burgess Reagent; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/psc.1276

upstream raw materials:

N-formyl-L-valine

N-Formyl-L-valine benzyl ester

benzyl alcohol

(S)-2-Isocyano-3-methyl-butyric acid benzyl ester