N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester
CAS No.:74024-23-0
Molecular Formula:C₄₇H₅₁NO₁₀
Molecular Weight:789.923
Hs Code.:

Synonyms:N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

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Technology Process of N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

There total 11 articles about N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 57224-63-2
methyl (2S,3R)-2-(benzyloxycarbonylamino)-3-hydroxybutyrate

: 74024-23-0
N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

Guidance literature:: trifluoromethylsulfonic anhydride; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85133-2

Reference yield: 64.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 57224-63-2
methyl (2S,3R)-2-(benzyloxycarbonylamino)-3-hydroxybutyrate

: 77942-96-2
N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-threonine methyl ester

: 74024-23-0
N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; -70 degC, 5 min; 20 min, r.t.;

Reference yield:

: 57224-63-2
methyl (2S,3R)-2-(benzyloxycarbonylamino)-3-hydroxybutyrate

: 166733-02-4
S-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-N,N,N',N'-tetramethyl-N''-phenylphosphorodiamidimidothioate

: 77942-96-2
N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-threonine methyl ester

: 74024-23-0
N-benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-threonine methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; 2,6-lutidinium p-toluenesulfonate; 4 A molecular sieve; In toluene; at 23 ℃; for 55h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)97729-3