2-[5-ethyl-5-(hydroxymethyl)-1,3-dioxan-2-yl]-2-methylpropan-1-ol

Base Information

• Chemical Name: 2-[5-ethyl-5-(hydroxymethyl)-1,3-dioxan-2-yl]-2-methylpropan-1-ol
• CAS No.: 59802-10-7
• Molecular Formula: C₁₁H₂₂O₄
• Molecular Weight: 218.293
• Mol file: 59802-10-7.mol

Synonyms:5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol

Chemical Property of 2-[5-ethyl-5-(hydroxymethyl)-1,3-dioxan-2-yl]-2-methylpropan-1-ol

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 123 °C
• Boiling Point: 323.1±17.0 °C(Predicted)
• PKA: 14.58±0.10(Predicted)
• Density: 1.055±0.06 g/cm3(Predicted)

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[5-ethyl-5-(hydroxymethyl)-1,3-dioxan-2-yl]-2-methylpropan-1-ol

There total 2 articles about 2-[5-ethyl-5-(hydroxymethyl)-1,3-dioxan-2-yl]-2-methylpropan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-3-hydroxypropionaldehyde (597-31-9) + 1,1,1-tri(hydroxymethyl)propane (77-99-6) → 5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol (59802-10-7)

Guidance literature:

In toluene; at 95 - 130 ℃; for 5h;

Reference yield:

→ 5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol (59802-10-7)

Guidance literature:

2,2-Dimethyl-3-hydroxy-propionaldehyd, 2-Hydroxymethyl-2-aethyl-propandiol-(1,3), p-Toluolsulfonsaeure (pH: 3) (Erwaermen);

DOI:10.1021/jo01034a518

Reference yield:

5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol (59802-10-7) + acryloyl chloride (814-68-6,25189-84-8) → 5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol diacrylate (87320-05-6)

Guidance literature:

With hydroquinone; trimethylamine; In chloroform; at 0 ℃; for 2h;

DOI:10.1021/bm100061z

upstream raw materials:

2,2-dimethyl-3-hydroxypropionaldehyde

1,1,1-tri(hydroxymethyl)propane

Downstream raw materials:

C₃₁H₄₄N₂O₁₀

5-ethyl-5-(hydroxymethyl)-β,β-dimethyl-1,3-dioxan-2-ethanol diacrylate