1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Base Information

• Chemical Name: 1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine
• CAS No.: 1006606-32-1
• Molecular Formula: C₂₈H₃₁NO₃
• Molecular Weight: 429.559

Synonyms:1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Chemical Property of 1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Chemical Property:

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Technology Process of 1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine

There total 1 articles about 1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-pyridinium triflate (1006606-19-4) → 1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine (1006606-32-1)

Guidance literature:

1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-pyridinium triflate; With sodium tetrahydroborate; cerium(III) chloride; In methanol; dichloromethane; at 0 ℃; for 0.333333h;

With acetic acid; In methanol; dichloromethane; Further stages.;

DOI:10.1002/anie.200704576

Reference yield: 100.0%

1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine (1006606-32-1) + 2-bromo-1-(bromomethyl)-3-methoxybenzene (128828-86-4) → Br(1-)*C36H39BrNO4(1+) (1187632-60-5)

Guidance literature:

In acetone; at 60 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.05.075

Reference yield: 100.0%

1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-1,2,3,6-tetrahydropyridine (1006606-32-1) + 3,5-dimethoxybenzyl bromide (877-88-3) → Br(1-)*C37H42NO5(1+) (1187632-62-7)

Guidance literature:

In acetone; at 60 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.05.075

upstream raw materials:

1-(3-methoxyphenethyl)-3,5-bis(3-methoxyphenyl)-pyridinium triflate

Downstream raw materials:

Br^(1-)*C₃₆H₃₉BrNO₄⁽¹⁺⁾

Br^(1-)*C₃₆H₄₀NO₄⁽¹⁺⁾

Br^(1-)*C₃₇H₄₂NO₅⁽¹⁺⁾

Br^(1-)*C₃₆H₃₉INO₄⁽¹⁺⁾

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