rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

Base Information

Chemical Name:rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal
CAS No.:103108-96-9
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

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Chemical Property of rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

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Technology Process of rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

There total 4 articles about rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-((1E,3E)-5-Hydroxy-3-methyl-penta-1,3-dienyl)-1,3-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

: 103108-96-9
rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

Guidance literature:: With manganese(IV) oxide; In diethyl ether; hexane; for 4h; Yield given; Ambient temperature;

Reference yield:

: 67192-51-2
trans-Aethyl-3-methyl-5-(2',6'-dimethyl-6'-aethoxycarbonyl-3'-oxo-1'-cyclohexenyl)-2,4-pentadienonat

: 103108-96-9
rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

Guidance literature:: Multi-step reaction with 4 steps

1: 84.8 percent / KOH / aq. ethanol / 6 h / Ambient temperature

2: diethylamine / tetrahydrofuran / 0.5 h / -5 °C

3: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 15 °C

4: MnO₂ / diethyl ether; hexane / 4 h / Ambient temperature

With manganese(IV) oxide; potassium hydroxide; sodium tetrahydroborate; diethylamine; In tetrahydrofuran; diethyl ether; ethanol; hexane; water;

Reference yield:

: 95524-25-7
rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienoic acid

: 103108-96-9
rac-(2E,4E)-3-methyl-5-(2,6-dimethyl-6-ethoxycarbonyl-3-oxo-1-cyclohexenyl)-2,4-pentadienal

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine / tetrahydrofuran / 0.5 h / -5 °C

2: NaBH₄ / tetrahydrofuran; H₂O / 0.5 h / 15 °C

3: MnO₂ / diethyl ether; hexane / 4 h / Ambient temperature

With manganese(IV) oxide; sodium tetrahydroborate; diethylamine; In tetrahydrofuran; diethyl ether; hexane; water;