3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

Base Information

Chemical Name:3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide
CAS No.:938448-49-8
Molecular Formula:C₂₁H₂₆N₂O₂S₂
Molecular Weight:402.582
Hs Code.:

3-benzylsulfanyl-<i>N</i>-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

Synonyms:3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

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Chemical Property of 3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

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Technology Process of 3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

There total 4 articles about 3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 6183-03-5
N-(S-benzyl-3-mercaptopropanoyl)glycine

: 22572-33-4
S-benzylcysteamine hydrochloride

: 938448-49-8
3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h;
DOI:10.1080/10426500600614824

Reference yield:

: 938448-46-5
(3-benzylsulfanyl-propionylamino)-acetic acid benzyl ester

: 938448-49-8
3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / AlCl₃; EtSH / 3 h / 0 - 20 °C

2: 66 percent / diisopropylethylamine; HBTU / dimethylformamide / 15 h / 20 °C

With aluminium trichloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; ethanethiol; In N,N-dimethyl-formamide;
DOI:10.1080/10426500600614824

Reference yield:

: 2899-66-3
3-(benzylthio)propanoic acid

: 938448-49-8
3-benzylsulfanyl-N-[(2-benzylsulfanyl-ethylcarbamoyl)-methyl]-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / diisopropylethylamine; HBTU / dimethylformamide / 16 h / 20 °C

2: 85 percent / AlCl₃; EtSH / 3 h / 0 - 20 °C

3: 66 percent / diisopropylethylamine; HBTU / dimethylformamide / 15 h / 20 °C

With aluminium trichloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; ethanethiol; In N,N-dimethyl-formamide;
DOI:10.1080/10426500600614824