4-Brom-benzylcyanamid

Base Information

• Chemical Name: 4-Brom-benzylcyanamid
• CAS No.: 98437-30-0
• Molecular Formula: C₈H₇BrN₂
• Molecular Weight: 211.061
• Mol file: 98437-30-0.mol

Synonyms:4-Brom-benzylcyanamid

Chemical Property of 4-Brom-benzylcyanamid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-Brom-benzylcyanamid

There total 1 articles about 4-Brom-benzylcyanamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-Brom-benzylcyanamid (98437-30-0)

Guidance literature:

4-Brom-benzylamin in Ae., Bromcyan in Ae., 20grad, 75 Min.;

DOI:10.1139/v61-130

Reference yield: 47.0%

4-Brom-benzylcyanamid (98437-30-0) + woollins’ reagent (122039-27-4) → N'-(4-bromobenzyl)carbamimidoyl(phenyl)phosphinodiselenoic acid (1186035-18-6) + N-(4-bromobenzyl)-2,4-diphenyl-2,5-dihydro-1,3,2,5-selenazadiphosphol-4-amine-2,5-diselenide

Guidance literature:

4-Brom-benzylcyanamid; woollins’ reagent; In toluene; for 10h; Inert atmosphere; Reflux;

With water; In toluene; at 90 ℃; Inert atmosphere; Reflux;

DOI:10.1016/j.tet.2009.05.056

Reference yield: 29.0%

4-Brom-benzylcyanamid (98437-30-0) + woollins’ reagent (122039-27-4) → N-(4-bromobenzyl)-2,4-diphenyl-2,5-dihydro-1,3,2,5-selenazadiphosphol-4-amine-2,5-diselenide

Guidance literature:

In toluene; at 130 ℃; for 10h; Inert atmosphere;

DOI:10.1016/j.tet.2009.05.056

Downstream raw materials:

N'-(4-bromobenzyl)carbamimidoyl(phenyl)phosphinodiselenoic acid