5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

Base Information

Chemical Name:5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide
CAS No.:1616924-85-6
Molecular Formula:C₃₀H₃₄ClN₃O₄
Molecular Weight:536.071
Hs Code.:

Synonyms:5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

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Chemical Property of 5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

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Technology Process of 5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

There total 7 articles about 5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616924-84-5
5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid [2-(tert-butyldimethylsilanyloxy)ethyl]cyclopropylmethylamide

: 1616924-85-6
5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 1h;

Reference yield:

: 532407-13-9
[2-(tert-butyldimethylsilanyloxy)ethyl]cyclopropylmethylamine

: 1616924-85-6
5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: 1616922-84-9
5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid

: 1616924-85-6
5-benzyloxy-2-[1-(4-chlorophenyl)cyclopentylmethyl]-6-hydroxypyrimidine-4-carboxylic acid cyclopropylmethyl(2-hydroxyethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; water; N,N-dimethyl-formamide;