(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

Base Information

Chemical Name:(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride
CAS No.:1446512-81-7
Molecular Formula:C₁₈H₁₆N₄O₅*ClH
Molecular Weight:404.81
Hs Code.:

Synonyms:(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

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Chemical Property of (S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

Chemical Property:

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Technology Process of (S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

There total 5 articles about (S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1446512-89-5
(S)-N-((4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenyloxy)carbonyl)-3-phenylsydnonimine

: 1446512-81-7
(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

Guidance literature:: (S)-N-((4-(2-((tert-butoxycarbonyl)amino)-3-methoxy-3-oxopropyl)phenyloxy)carbonyl)-3-phenylsydnonimine; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; water; at 0 - 20 ℃; for 1h; pH=2;
DOI:10.1039/c3ob41047a

Reference yield:

: 3009-97-0
N-phenylglycinonitrile

: 1446512-81-7
(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

1.2: 0.25 h / 20 °C

2.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

3.1: acetonitrile / 18 h / Reflux

4.1: sodium hydroxide / water; tetrahydrofuran / 20 °C

4.2: 1 h / 0 - 20 °C / pH 2

With triethylamine; sodium hydroxide; isopentyl nitrite; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1039/c3ob41047a

Reference yield:

: 62-53-3
aniline

: 1446512-81-7
(S)-N-((4-(2-amino-2-carboxyethyl)phenyl)carbonyl)-3-phenylsydnonimine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; sodium iodide / acetone / 12 h / 20 °C / Darkness

2.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

2.2: 0.25 h / 20 °C

3.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

4.1: acetonitrile / 18 h / Reflux

5.1: sodium hydroxide / water; tetrahydrofuran / 20 °C

5.2: 1 h / 0 - 20 °C / pH 2

With potassium carbonate; triethylamine; sodium iodide; sodium hydroxide; isopentyl nitrite; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c3ob41047a