Technology Process of C28H29N3O7S2
There total 7 articles about C28H29N3O7S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H27N3O6S2;
With
9-BBN;
In
tetrahydrofuran;
at 23 ℃;
With
dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; ethanol; water;
at 0 - 23 ℃;
DOI:10.1016/j.tetlet.2010.11.074
- Guidance literature:
-
C28H29N3O7S2;
With
pyridine; trichlorophosphate;
at 0 - 23 ℃;
Inert atmosphere;
With
9-borabicyclo[3.3.1]nonane dimer;
In
tetrahydrofuran;
at 23 ℃;
for 10h;
Inert atmosphere;
With
sodium hydroxide; dihydrogen peroxide;
In
tetrahydrofuran; ethanol; water;
at 0 - 23 ℃;
DOI:10.1021/ja804738b
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: palladium on carbon; hydrogen / methanol / 23 °C
2.1: triethylamine / dichloromethane / 0 - 23 °C
3.1: pyridinium perbromide hydrobromide / dichloromethane / 0 - 23 °C
4.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 100 °C
5.1: trichlorophosphate / pyridine / 0 - 23 °C
6.1: 9-BBN / tetrahydrofuran / 23 °C
6.2: 0 - 23 °C
With
9-BBN; tetrakis(triphenylphosphine) palladium(0); pyridinium perbromide hydrobromide; palladium on carbon; hydrogen; triethylamine; trichlorophosphate;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2010.11.074
