C₂₃H₃₂O₅

Base Information

Chemical Name:C₂₃H₃₂O₅
CAS No.:1111685-26-7
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>5</sub>

Synonyms:C₂₃H₃₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₂O₅

Chemical Property:

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Technology Process of C₂₃H₃₂O₅

There total 7 articles about C₂₃H₃₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1111685-24-5
ethyl 8-hydroxy-1-oxaspiro[4,5]decane-8-carboxylate

: 4408-60-0
2-mesitylacetic acid

: 1111685-26-7
C₂₃H₃₂O₅

Guidance literature:: 2-mesitylacetic acid; With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 90 ℃; for 1h;

ethyl 8-hydroxy-1-oxaspiro[4,5]decane-8-carboxylate; In toluene; at 90 ℃; for 8h;

With sodium hydroxide; In water;

Reference yield:

: 90214-47-4
4-(3-hydroxypropyl)-4-hydroxy-cyclohexanone ethylene ketal

: 1111685-26-7
C₂₃H₃₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 °C

2.1: hydrogenchloride / tetrahydrofuran; water / 80 °C

3.1: water / 0.5 h / 20 - 28 °C

3.2: 20 °C

4.1: hydrogenchloride / -20 - 20 °C

4.2: 3 h / Cooling with ice

5.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 1 h / 90 °C

5.2: 8 h / 90 °C

With hydrogenchloride; thionyl chloride; methanesulfonyl chloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; toluene;

Reference yield:

: 429691-42-9
8-allyl-1,4-dioxaspiro[4.5]decan-8-ol

: 1111685-26-7
C₂₃H₃₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 °C

2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 80 °C

4.1: water / 0.5 h / 20 - 28 °C

4.2: 20 °C

5.1: hydrogenchloride / -20 - 20 °C

5.2: 3 h / Cooling with ice

6.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 1 h / 90 °C

6.2: 8 h / 90 °C

With hydrogenchloride; thionyl chloride; dimethylsulfide borane complex; methanesulfonyl chloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; toluene;