C₂₇H₂₉NO₃

Base Information

Chemical Name:C₂₇H₂₉NO₃
CAS No.:1453222-94-0
Molecular Formula:C₂₇H₂₉NO₃
Molecular Weight:415.532
Hs Code.:

C<sub>27</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₇H₂₉NO₃

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Chemical Property of C₂₇H₂₉NO₃

Chemical Property:

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Technology Process of C₂₇H₂₉NO₃

There total 4 articles about C₂₇H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1629-58-9
4-penten-3-one

: 1453222-60-0
C₂₂H₂₁NO₂

: 1453222-94-0
C₂₇H₂₉NO₃

Guidance literature:: 4-penten-3-one; C₂₂H₂₁NO₂; With tin(IV) chloride; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere; Molecular sieve;

diastereoselective reaction;
DOI:10.1021/ol402254p

Reference yield:

: 1453223-20-5
C₂₂H₂₁NO₂

: 1453222-94-0
C₂₇H₂₉NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: CSA / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

2: acetonitrile / 16 h / 125 °C / Inert atmosphere; Sealed tube

3: tin(IV) chloride / dichloromethane / 1 h / -78 °C / Inert atmosphere; Molecular sieve

With tin(IV) chloride; In dichloromethane; acetonitrile; 3: |Diels-Alder Cycloaddition;
DOI:10.1021/ol402254p

Reference yield:

: 1453223-21-6
C₂₂H₂₁NO₂

: 1453222-94-0
C₂₇H₂₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 16 h / 125 °C / Inert atmosphere; Sealed tube

2: tin(IV) chloride / dichloromethane / 1 h / -78 °C / Inert atmosphere; Molecular sieve

With tin(IV) chloride; In dichloromethane; acetonitrile; 2: |Diels-Alder Cycloaddition;
DOI:10.1021/ol402254p