3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Base Information

Chemical Name:3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole
CAS No.:108470-81-1
Molecular Formula:C₁₂H₁₃NO₃S
Molecular Weight:251.306
Hs Code.:

3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopent<d>isoxazole

Synonyms:3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Suppliers and Price of 3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

There total 3 articles about 3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 116503-02-7
3a,5,6,6a-tetrahydro-3-(phenylthio)-4H-cyclopentisoxazole

: 108470-81-1
3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00257a036

Reference yield:

: 60595-16-6
(phenylthio)nitromethane

: 108470-81-1
3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / phenylisocyanate, triethylamine / benzene / 1.) 25 deg C, 30 min, 2.) 45 deg C, 12 h

2: 71 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 1 h / Ambient temperature

With phenyl isocyanate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1021/jo00257a036

Reference yield:

: 142-29-0
cyclopentene

: 108470-81-1
3a,5,6,6a-tetrahydro-3-(phenylsulfonyl)-4H-cyclopentisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / phenylisocyanate, triethylamine / benzene / 1.) 25 deg C, 30 min, 2.) 45 deg C, 12 h

2: 71 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 1 h / Ambient temperature

With phenyl isocyanate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1021/jo00257a036