6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

Base Information

Chemical Name:6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole
CAS No.:1056263-77-4
Molecular Formula:C₂₁H₁₆BrFN₂O₂
Molecular Weight:427.273
Hs Code.:

Synonyms:6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

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Chemical Property of 6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

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Technology Process of 6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

There total 1 articles about 6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885519-21-1
6-bromo-4-methoxy-1H-indazole

: 133057-83-7
4-benzyloxy-3-fluorophenylboronic acid

: 1056263-77-4
6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

Guidance literature:: With pyridine; copper diacetate; In dichloromethane; at 20 ℃; for 120h; Molecular sieve;

Reference yield:

: 1056263-77-4
6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

: 1056261-91-6
6-bromo-1-(3-fluoro-4-hydroxyphenyl)-1H-indazol-4-ol

Guidance literature:: 6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole; With water; hydrogen bromide; at 130 ℃; for 3h;

With sodium hydroxide; water; In ethyl acetate; at 20 ℃; pH=7;

Reference yield:

: 1056263-77-4
6-bromo-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

: 1056261-99-4
6-ethenyl-1-(3-fluoro-4-hydroxyphenyl)-1H-indazol-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; hydrogen bromide / 3 h / 130 °C

1.2: 20 °C / pH 7

2.1: dichlorobis(tri-O-tolylphosphine)palladium / 1,2-dimethoxyethane / 90 °C

With water; hydrogen bromide; dichlorobis(tri-O-tolylphosphine)palladium; In 1,2-dimethoxyethane;