methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate

Base Information

• Chemical Name: methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate
• CAS No.: 235757-79-6
• Molecular Formula: C₃₁H₃₁NO₈S
• Molecular Weight: 577.655

Synonyms:methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate

Chemical Property of methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate

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Technology Process of methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate

There total 1 articles about methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

thiophenol (108-98-5) + methyl 6-((3S)-3-<(5S,4R)-5-<2-aza-2-(phenylmethoxy)vinyl>-2,2-dimethyl(1,3-dioxolan-4-yl)>-3-hydroxyprop-1-ynyl)-2H-benzo1,3-dioxolene-5-carboxylate → methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate (235757-79-6)

Guidance literature:

In toluene; at 21 - 27 ℃; for 5h; Irradiation;

DOI:10.1021/ja9826688

Reference yield: 86.0%

methyl 6-<(3aS,4R,7R,7aR)-7-hydroxy-2,2-dimethyl-4-<(phenylmethoxy)amino>-6-phenylthio-2,3,4,7,3a,7a-hexahydro-1,3-dioxainden-5-yl>-2H-benzo1,3-dioxolane-5-carboxylate (235757-79-6) → (2S,5aS,2aR,5bR)-2-hydroxy-4,4-dimethyl-2,6,2a,5a,5b-pentahydro-10H-1,3-dioxolano<4,5-j>1,3-dioxolano<4,5-c>phenanthridin-7-one (235757-86-5) + (5aS,2R,2aR,5bR)-2-hydroxy-4,4-dimethyl-1-phenylthio-2,6,2a,5a,5b-pentahydro-10H-1,3-dioxolano<4,5-j>1,3-dioxolano<4,5-c>phenanthridin-7-one

Guidance literature:

With samarium diiodide; In tetrahydrofuran; for 42h; Ambient temperature;

DOI:10.1021/ja9826688

upstream raw materials:

thiophenol

Downstream raw materials:

(2S,5aS,2aR,5bR)-2-hydroxy-4,4-dimethyl-2,6,2a,5a,5b-pentahydro-10H-1,3-dioxolano<4,5-j>1,3-dioxolano<4,5-c>phenanthridin-7-one

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