Technology Process of C19H24O5
There total 7 articles about C19H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
Reflux;
DOI:10.1039/c3ra45419c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: AD-mix β / tert-butyl alcohol; water / 0 °C
2: triethylamine; dmap / dichloromethane / 0 - 20 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
With
dmap; lithium aluminium tetrahydride; AD-mix β; triethylamine;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
1: |Sharpless Dihydroxylation;
DOI:10.1039/c3ra45419c
- Guidance literature:
-
Multi-step reaction with 7 steps
1: tetrahydrofuran / 0 - 20 °C
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; dichloromethane / 0 - 20 °C
3: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / -40 °C
4: sodium hydride / tetrahydrofuran / 0 - 20 °C
5: AD-mix β / tert-butyl alcohol; water / 0 °C
6: triethylamine; dmap / dichloromethane / 0 - 20 °C
7: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
With
dmap; lithium aluminium tetrahydride; dimethylsulfide borane complex; AD-mix β; sodium hydride; triethylamine; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
5: |Sharpless Dihydroxylation;
DOI:10.1039/c3ra45419c
