Ru2DPB(triphenylphosphine)2(μ-hydrazine)

Base Information

• Chemical Name: Ru2DPB(triphenylphosphine)2(μ-hydrazine)
• CAS No.: 107081-49-2
• Molecular Formula: C₁₁₂H₁₁₀N₁₀P₂Ru₂
• Molecular Weight: 1860.26
• Mol file: 107081-49-2.mol

Synonyms:Ru2DPB(triphenylphosphine)2(μ-hydrazine)

Chemical Property of Ru2DPB(triphenylphosphine)2(μ-hydrazine)

Chemical Property:

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Technology Process of Ru2DPB(triphenylphosphine)2(μ-hydrazine)

There total 1 articles about Ru2DPB(triphenylphosphine)2(μ-hydrazine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

{(1,8-bis{5-(2,8,13,17-tetraethyl-3,7,12,18-tetramethyl)porphyrin}biphenylene tetra-anion)Ru2(triphenylphosphine)2} (107081-53-8) → Ru2DPB(triphenylphosphine)2(μ-hydrazine) (107081-49-2)

Guidance literature:

With hydrazine; In toluene; dissolution of Ru-complex in toluene (drybox), addn. of 2 drops of N2H4, stirring for 5 h at room temp.; column chromy. (alumina, neutral, activity I) evapn. to dryness, drying under high vac.; elem. anal.;

upstream raw materials:

{(1,8-bis{5-(2,8,13,17-tetraethyl-3,7,12,18-tetramethyl)porphyrin}biphenylene tetra-anion)Ru₂(triphenylphosphine)2}