2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

Base Information

Chemical Name:2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester
CAS No.:177587-72-3
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

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Chemical Property of 2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

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Technology Process of 2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

There total 1 articles about 2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17145-91-4
triethyl 2-ethylphosphonoacetate

: 149428-73-9
4-methoxy-3-(2-phenylethoxy)-benzaldehyde

: 177587-72-3
2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

Guidance literature:: triethyl 2-ethylphosphonoacetate; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 0.5h;

4-methoxy-3-(2-phenylethoxy)-benzaldehyde; In 1,2-dimethoxyethane; for 2h; Heating;
DOI:10.1021/jm990135j

Reference yield:

: 177587-72-3
2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

: 177587-73-4
ethyl 3-[4-methoxy-3-(2-phenylethoxy)phenyl]-2-ethylpropionate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm990135j

Reference yield:

: 177587-72-3
2-[1-(4-Methoxy-3-phenethyloxy-phenyl)-meth-(E)-ylidene]-butyric acid ethyl ester

: 1-(4-methoxy-3-phenethyloxy-benzyl)-propylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: H₂ / 5 percent Pd/C / ethanol

2.1: aq. KOH / ethanol

3.1: diphenyl phosphorazidate, Et₃N / benzene / 2 h / Heating

3.2: 20 h / Heating

4.1: CF₃CO₂H / CH₂Cl₂ / 1.5 h / 20 °C

With potassium hydroxide; diphenyl phosphoryl azide; hydrogen; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; benzene; 1.1: Hydrogenation / 2.1: Hydrolysis / 3.1: modified Curtius reaction / 3.2: Alkylation / 4.1: Hydrolysis;
DOI:10.1021/jm990135j